Abstract
ULTRAVIOLET ASSAY OF METOCLOPRAMIDE. HCL IN PHARMACEUTICAL FORMULATIONS APPLICATION TO CONTENT UNIFORMITY TESTING

Nief Rahman Ahmed*, Mohammad Jassim Essa and Ahmad Khaled Hamdoon

ABSTRACT

A simple, accurate, precise, rapid, economical and sensitive ultra violet spectrophotometric method has been developed for the estimation of metoclopramide. HCL in pharmaceutical preparations and environmental wastewater samples, which shows maximum absorbance at 310 nm in distilled water. Beer's law was obeyed in the range of 2-25 μ g/ ml, with molar absorptivity of 1.25X104 L.mol-1.cm-1, relative standard deviation of the method was less than 1.8%, and accuracy (average recovery %) was 100 ± 1.0. The method was successfully applied to the estimation of metoclopramide. HCL in pharmaceutical formulations, content uniformity testing and industrial wastewater samples The proposed method was validated by sensitivity and precision which proves suitability for the routine analysis of metoclopramide. HCL in true samples.

Keywords: Metoclopramide. HCL, Ultra violet, Pharmaceutical preparations.


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